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Sulphonamide of Glibenclamide

Sulphonamide of Glibenclamide

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Sulphonamide of Glibenclamide


TEST

SPECIFICATION


Description

An Almost white to slight yellow  crystalline powder.


Solubility

Soluble in N,N- Dimethyl formamide,
Very slightly soluble in ethanol.
Practically insoluble in chloroform.


IR Spectrum

Must Comply


Melting Range

204 C to 212 C


LOD

NMT 0.5  % w/w


Related Substance

3,5-Dichloro Analog  NMT 0.2  %
Sulfonamide Diner     NMT 1.0  %


Assay

97 % to 101  %


Residual Solvents

1.Methanol NMT 3000 PPM
2. Acetone NMT 3000 PPM
3. Ethylene Di chloride 1870 PPM